Experiment
Title
Vis-NIR and Mid-IR reflectance spectra, Mid-IR transmission and Raman spectra of several preparations of the Oued Chebeika 002 meteorite (CI chondrite)
DOI
10.26302/SSHADE/EXPERIMENT_LB_20241211_001
Data reference
Bonal, Lydie; Beck, Pierre; Poch, Olivier (2024): Vis-NIR and Mid-IR reflectance spectra, Mid-IR transmission and Raman spectra of several preparations of the Oued Chebeika 002 meteorite (CI chondrite). SSHADE/GhoSST (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_LB_20241211_001
Publications
Type(s)
laboratory measurement
Description
Mid-IR and Vis-NIR reflectance spectra (i = 0°, e = 30°) - recorded with two different instruments - of raw chips and powdered sample, Mid-IR transmission of matrix fragments pressed on diamonds, and Raman emission spectra of matrix fragments pressed on glass slide of the Oued Chebeika 002 meteorite (CI chondrite)
Number of spectra
20
Variable type(s)
  • spectrum type
  • sample composition
Comments
measurements of several preparations of Oued Chebeika 002 with different techniques and instruments
Instrument
SHINE Spectro-Gonio bidirectional reflection Vis-NIR
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
Vis, NIR
Valid spectral range(s)
Min - Max (nm) Sampling (nm) Resolution (nm) Position accuracy (nm) Absorption edge
#1 1000.0 - 1590.0 10.0 9.5
#2 1600.0 - 2830.0 10.0 19.0
#3 2840.0 - 4200.0 10.0 39.0
Comments
spectra were recordred in the 500-4000 nm range but there are some issues with data below 550 nm
Observation geometry
bidirectional
Observation mode
fixed angles
Incidence angle
0.0°
Emergence angle
30.0°
Azimuth angle
0.0°
Phase angle
30.0°
Resolution illumination
5.8°
Resolution observation
4.1°
Illumination
Observation
Comments
partial polarization variable with wavelength (from monochromator grating)
Observation mode
single spot
Comments
samples were illuminated with a monochromatic beam <= 1.7 mm in diameter
Instrument
SHADOWS Spectro-Gonio bidirectional reflection Vis-NIR
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
Vis, NIR
Valid spectral range(s)
Min - Max (nm) Sampling (nm) Resolution (nm) Position accuracy (nm) Absorption edge
#1 1000.0 - 1590.0 10.0 9.5
#2 1600.0 - 2830.0 10.0 19.0
#3 2840.0 - 4200.0 10.0 39.0
Comments
spectra were recordred in the 500-4000 nm range but there are some issues with data below 550 nm
Observation geometry
bidirectional
Observation mode
fixed angles
Incidence angle
0.0°
Emergence angle
30.0°
Azimuth angle
0.0°
Phase angle
30.0°
Resolution illumination
5.8°
Resolution observation
4.1°
Illumination
Observation
Comments
partial polarization variable with wavelength (from monochromator grating)
Observation mode
single spot
Comments
samples were illuminated with a monochromatic beam <= 1.7 mm in diameter
Instrument
Brucker Vertex 70 #2 – reflection Mid-IR
Sample holder
aluminum sample holder
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
NIR, MIR
Valid spectral range(s)
Min - Max (μm) Sampling (μm) Resolution (μm) Position accuracy (μm) Absorption edge
#1 2.3 - 18.0 0.00056
Comments
measured from 0.54 μm to 2.3 μm with SHINE and from 2.3 to 18 μm with Vertex70v instrument
Observation geometry
biconical
Observation mode
fixed angles
Incidence angle
0.0°
Emergence angle
30.0°
Observation mode
single spot
Spatial resolution
1.0 mm
Instrument
Brucker Vertex 70 + Hyperion 3000 – micro-transmission Mid-IR
Sample holder
The diamond windows were loaded into a cell, enabling temperature up to 300°C under vacuum (from 10-4 mbar down to 10-7 mbar). Optical access is permitted from both sides of the cell through KBr windows, thus enabling measurements in transmission.
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
MIR
Valid spectral range(s)
Min - Max (cm1) Sampling (cm1) Resolution (cm1) Position accuracy (cm1) Absorption edge
#1 600.0 - 4000.0 1.929 4.0 0.05
Observation mode
single spot
Spots number
1
Objective type
x15
Pixels number
1 x 1
Image size
40.0 x 40.0 μm
Spatial resolution
3.0 ± 1.0 μm
Comments
the typical size of the spot on the sample was 40 x 40 µm²
Instrument
Micro-Raman LabRam HR800 - 532 nm
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
MIR, FIR
Valid spectral range(s)
Min - Max (cm1) Sampling (cm1) Resolution (cm1) Position accuracy (cm1) Absorption edge
#1 555.0 - 2171.0 1.7 0.2
Filters
Type Center/Edge (cm1) Width (cm1) Place
#1 532.3 nm edge filter 100.0
Comments
Sampling varies from 1.7 to 1.4 cm1 in the 555-2170 cm1 range
Observation geometry
confocal
Observation mode
fixed angles
Incidence angle
0.0°
Emergence angle
0.0°
Observation mode
single spot
Objective type
x100
Spatial resolution
1.0 μm
Date begin - end
2024-11-25 - 2024-12-15

Versions

Release date
2025-03-28 10:26:10 UTC+0000
Version (Date)
#1 (2025-03-28 10:26:10 UTC+0000, Updated: 2025-03-28 10:26:10 UTC+0000)