- Title
- Pd K edge XAS fluorescence of 1 wt.% Pd/SiO2 at RT under He or H2 (after heating at 300C under H2)
- DOI
- 10.26302/SSHADE/EXPERIMENT_SOC_20170316_001
- Data reference
- Ould-Chikh, Samy (2017): Pd K edge XAS fluorescence of 1 wt.% Pd/SiO2 at RT under He or H2 (after heating at 300C under H2). SSHADE/FAME (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_SOC_20170316_001
- Publications
- Database(s)
- Experimentalists
- Type(s)
- laboratory measurement
- Number of spectra
- 3
- Comments
- These data were acquired on the BM30 beamline in the frame of the 30-02-1111 proposal.
- Variable type(s)
-
- other
- Instrument
- X-ray Absorption Spectroscopy measured in fluorescence mode
- Sample holder
- FAME catalysis cell, see Aguilar-Tapia et al., Rev. Sci. Instrum., 2018
- Standard medium
- unknown
- Observation mode
- spectrum
- Spectral range type(s)
- hard X
- Valid spectral range(s)
-
Min - Max ($eV$) Sampling ($eV$) Resolution ($eV$) Position accuracy ($eV$) Absorption edge #1 24201.0 - 25204.0 1.25 $Pd$ (K: 24.3503 $keV$) - Comments
- The resolution in the above table is the resolution given by the monochromator. The energy was calibrated by measuring the absorption edge of a reference: Pd metallic foil (first maximum of the derivative set at 24350 eV).
Definition: emergence angle is positive with origin at nadir. Azimuth origin (increasing clockwise) is arbitrary.
- Observation geometry
- directional
- Observation mode
- fixed angles
- Comments
- Emitted x-rays are collected in a solid angle directed at 90 degrees from the incident beam.
- Observation mode
- single spot
- Date begin - end
- 2017-03-16 - 2017-03-22
Versions
- Release date
- 2021-07-20 12:05:32 UTC+0000
- Version (Date)
- #1 (2021-07-20 12:05:32 UTC+0000, Updated: 2021-07-20 12:05:32 UTC+0000)