Spectrum

Near-infrared reflectance spectra at 169K of Ammonium hydrogen sulphate-II [(NH4)HSO4] powder with 125-150µm grain size

Title
Near-infrared reflectance spectra at 169K of Ammonium hydrogen sulphate-II [(NH4)HSO4] powder with 125-150µm grain size
DOI
10.26302/SSHADE/EXPERIMENT_BS_20241810_001
Data reference
Fastelli, Maximiliano; Schmitt, Bernard; Beck, Pierre; Poch, Olivier (2021): Near-infrared reflectance spectra at low temperature (110-290K) of Ammonium hydrogen sulphate-I, -II and -III [(NH4)HSO4] powder with 125-150µm grain size. SSHADE/CSS (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_BS_20241810_001
Publications
Experiment type
laboratory measurement
Type
reflectance factor
Intensity unit
no unit
Instrument
SHINE Spectro-Gonio bidirectional reflection Vis-NIR
Sample holder
Cylindrical aluminum sample holder placed in the isothermal CarboN-IR cryogenic cell with two saphire windows.
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
NIR
Valid spectral range(s)
Min - Max ($nm$) Sampling ($nm$) Resolution ($nm$) Position accuracy ($nm$) Absorption edge
#1 1000.0 - 1600.0 10.0 7.55 1.0
#2 1610.0 - 2830.0 10.0 15.3 1.5
#3 2840.0 - 3200.0 10.0 31.0 3.0
#4 3220.0 - 4180.0 20.0 30.9 3.0
#5 4340.0 - 4600.0 20.0 30.75 3.0
Scan number
10
Comments
A series of high pass filters is used to remove high orders of the gratings
Observation geometry
bidirectional
Observation mode
fixed angles
Incidence angle
0.0°
Emergence angle
20.0°
Azimuth angle
0.0°
Phase angle
20.0°
Resolution illumination
5.8°
Resolution observation
4.1°
Comments
'Gognito' illumination attachment with focused beam
Illumination
Observation
Comments
Partial polarization variable with wavelength (from the 3 monochromator gratings used)
Observation mode
single spot
Resolutions
7.5 $mm$
Name
Ammonium hydrogen sulphate powder (Phase II) - grains: 125-150µm
Changes
fully transformed to phase II of Ammonium hydrogen sulphate during warming to 162K
Experiment
Near-infrared reflectance spectra at low temperature (110-290K) of Ammonium hydrogen sulphate-I, -II and -III [(NH4)HSO4] powder with 125-150µm grain size
Date begin
2021-11-06 18:24:00
Release date
2024-09-28 04:57:29 UTC+0000
Version (Date)
#1 (2024-09-28 04:57:29 UTC+0000, Updated: 2024-09-28 04:57:29 UTC+0000)
History
Date Mode Version Status Comments
2024-09-22 21:32:44 UTC+0000 first import #1 valid version
Analysis
Raw bidirectional reflectance spectrum calibrated: 1) with "Spectralon 99%" measured under same geometry using its absolute BRDF (1000-1300nm) and 2) with "Infragold" using its relative spectral reflectance (1300-4800nm). The multiple reflections from the two saphire windows of the cell are corrected by a calibration function taking into account the sample surface reflectance. Only minor residual water vapor line is observed.
Quality flag
4
Validator(s)