Sample
Name
Ammonium hydrogen sulphate powder (Phase III) - grains: 125-150µm
Date
2021-11-04
Provider
Alfa Aesar
Thickness
4.5 $\pm$ 0.1 $mm$
Diameter
18.0 $mm$
Volume
1145.0 $mm^3$
Mass
1.165 $\pm$ 0.005 $g$
Surface roughness
smooth
Sample changes
fully transformed to phase III of Ammonium hydrogen sulphate during warming to 270K
Substrate material
Aluminium
Substrate comments
cylindrical hole, diameter: 18 mm, depth: 4.5 mm
Comments
slightly smoothing the surface by sliding a flat aluminium plate
Temperature
273.0 $\pm$ 0.5 $K$
Temperature max
295.0 $\pm$ 3.0 $K$
Comments
recording of the spectrum takes 82 min
Type
molecular gas
Fluids
Fluid temperature
273.0 $K$
Fluid pressure
10.0 $mbar$
Comments
high purity N2 gas
Number
1
Layers