- DOI
- 10.26302/SSHADE/EXPERIMENT_FS_20201007_001
- Data reference
- Stellato, Francesco; Morante, Silvia; Proux, Olivier; Consalvi, Valerio (2020): Co K edge XAS fluorescence of CoSO4 in buffer for the study of the Iron binding site in the mature and C-terminal regions of wild-type and mutant human frataxin.. SSHADE/FAME (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_FS_20201007_001
- Publications
- Database
- Experimentalists
- Experiment type
- laboratory measurement
- Type
- fluorescence emission
- Intensity unit
- AU
- Instrument
- X-ray Absorption Spectroscopy measured in fluorescence mode
- Sample holder
- Oxford-ILL orange cryostat
- Standard medium
- unknown
- Observation mode
- spectrum
- Spectral range type(s)
- hard X
- Excitation wavelength
- hard X
- Valid spectral range(s)
-
Min - Max ($eV$) Sampling ($eV$) Resolution ($eV$) Position accuracy ($eV$) Absorption edge #1 7579.0 - 8562.0 0.395 $Co$ (K: 7.7089 $keV$) - Comments
- The resolution in the above table is the resolution given by the monochromator. The energy was calibrated by measuring the absorption edge of a reference: Fe metallic foil (first maximum of the derivative set at 7112 eV).
Definition: emergence angle is positive with origin at nadir. Azimuth origin (increasing clockwise) is arbitrary.
- Observation geometry
- directional
- Observation mode
- fixed angles
- Comments
- Emitted x-rays are collected in a solid angle directed at 90 degrees from the incident beam.
- Observation mode
- averaged
- Experiment
- Co K edge XAS fluorescence of CoSO4 in buffer for the study of the Iron binding site in the mature and C-terminal regions of wild-type and mutant human frataxin.
- Date begin
- 2020-10-07
- Release date
- 2022-11-02 10:43:09 UTC+0000
- Version (Date)
- #1 (2022-11-02 10:43:09 UTC+0000, Updated: 2022-11-02 10:43:09 UTC+0000)
- History
-
Date Mode Version Status Comments 2020-10-29 13:32:03 UTC+0000 first import #1 valid version
- Analysis
- raw averaged spectra