Ni K edge XAS fluorescence of square planar Nickel(II) with Ni-S4 coordination at 16K
- Title
- Ni K edge XAS fluorescence of square planar Nickel(II) with Ni-S4 coordination at 16K
- DOI
- 10.26302/SSHADE/EXPERIMENT_GV_20160403_001
- Data reference
- Veronesi, Giulia; Cavazza, Christine; Proux, Olivier (2016): Ni K edge XAS fluorescence of square planar Nickel(II) with Ni-N2S2 or Ni-S4 coordination at 16K. SSHADE/FAME (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_GV_20160403_001
- Publications
- Database
- Experimentalists
- Experiment type
- laboratory measurement
- Type
- fluorescence emission
- Intensity unit
- AU
- Instrument
- X-ray Absorption Spectroscopy measured in fluorescence mode
- Sample holder
- Oxford-ILL orange cryostat
- Standard medium
- unknown
- Observation mode
- spectrum
- Spectral range type(s)
- hard X
- Excitation wavelength
- hard X
- Valid spectral range(s)
-
Min - Max ($eV$) Sampling ($eV$) Resolution ($eV$) Position accuracy ($eV$) Absorption edge #1 8099.0 - 9302.0 0.427 $Ni$ (K: 8.3328 $keV$) - Comments
- The resolution in the above table is the resolution given by the monochromator. The energy was calibrated by measuring the absorption edge of a reference: Ni metallic foil (first maximum of the derivative set at 8333 eV).
Definition: emergence angle is positive with origin at nadir. Azimuth origin (increasing clockwise) is arbitrary.
- Observation geometry
- directional
- Observation mode
- fixed angles
- Comments
- Emitted x-rays are collected in a solid angle directed at 90 degrees from the incident beam.
- Observation mode
- averaged
- Experiment
- Ni K edge XAS fluorescence of square planar Nickel(II) with Ni-N2S2 or Ni-S4 coordination at 16K
- Date begin
- 2016-04-03
- Release date
- 2019-11-19 12:34:23 UTC+0000
- Version (Date)
- #1 (2019-11-19 12:34:23 UTC+0000, Updated: 2019-11-22 07:41:50 UTC+0000)
- History
-
Date Mode Version Status Comments 2019-11-19 12:32:37 UTC+0000 first import #1 valid version
- Analysis
- raw averaged spectra