Ni K edge XAS fluorescence of Ni NTA(CysNH_2)_3 at pH=7.5 and at 10K | FAME

Spectrum

Ni K edge XAS fluorescence of $Ni NTA(CysNH_2)_3$ at pH=7.5 and at 10K

Title: Ni K edge XAS fluorescence of $Ni NTA(CysNH_2)_3$ at pH=7.5 and at 10K

Draw options

Draw line: Fill area:
Line width:
Fill opacity:
Colors: Invert:

Range:

Saturation:
Lightness:

Data

Unit: Range: Valid spectral range(s): 65330907.3704011 - 74082022.7403869 eV

X Axis

Scale: Inverted:

Y Axis

Scale:

Legend

Position: Visibility:

References

DOI

10.26302/SSHADE/EXPERIMENT_JD_20171122_001

Data reference

Pécaut, Jacques; Domergue, Jérémy; Duboc, Carole; Delangle, Pascale (2017): Ni K edge XAS transmission and XAS fluorescence of Ni complexes (with cysteine-rich ligands) at 10K. SSHADE/FAME (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_JD_20171122_001

Publications

Domergue et al., 2019, Inorg. Chem., 58, 12775 - 12785

Owner

Database

FAME

Experimentalists

Spectrum type

Experiment type: laboratory measurement
Type: fluorescence emission
Intensity unit: AU

Instrument #1

Instrument: X-ray Absorption Spectroscopy measured in fluorescence mode
Sample holder: Oxford-ILL orange cryostat

Spectral parameters

Standard medium

unknown

Observation mode

spectrum

Spectral range type(s)

hard X

Excitation wavelength

hard X

Valid spectral range(s)

	Min - Max ($eV$)	Sampling ($eV$)	Resolution ($eV$)	Position accuracy ($eV$)	Absorption edge
#1	8100.0 - 9185.0		0.427		$Ni$ (K: 8.3328 $keV$)

Comments

The resolution in the above table is the resolution given by the monochromator. The energy was calibrated by measuring the absorption edge of a reference: Ni metallic foil (first maximum of the derivative set at 8333 eV).