- Title
- Pb L3 edge XAS fluorescence of lead(II) solution at hydrothermal conditions: 800 bar, 30 to 489°C
- DOI
- 10.26302/SSHADE/EXPERIMENT_DT_20170215_001
- Data reference
- Testemale, Denis; Brugger, Joel; Etschmann, Barbara; Liu, Weihua (2017): Pb L3 edge XAS fluorescence of lead(II) solution at hydrothermal conditions: 800 bar, 30 to 489°C. SSHADE/FAME (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_DT_20170215_001
- Publications
- Database(s)
- Experimentalists
- Type(s)
- laboratory measurement
- Description
- Chloride, bromide and bisulfide bearing solutions; temperature varying from 30 to 489°C
- Number of spectra
- 42
- Comments
- These data were acquired on the BM30 beamline in the frame of the ES-451 proposal.
- Variable type(s)
-
- sample composition
- temperature
- Instrument
- X-ray Absorption Spectroscopy measured in fluorescence mode
- Sample holder
- Institut Néel autoclave, see Testemale et al., Rev. Sci. Instrum., 2005.
- Standard medium
- unknown
- Observation mode
- spectrum
- Spectral range type(s)
- hard X
- Valid spectral range(s)
-
Min - Max ($eV$) Sampling ($eV$) Resolution ($eV$) Position accuracy ($eV$) Absorption edge #1 12847.0 - 13416.0 0.668 $Pb$ (L3: 13.0352 $keV$) - Comments
- The resolution in the above table is the resolution given by the monochromator. The energy was calibrated by measuring the absorption edge of a reference: Pb metallic foil (first maximum of the derivative set at 13035 eV).
Definition: emergence angle is positive with origin at nadir. Azimuth origin (increasing clockwise) is arbitrary.
- Observation geometry
- directional
- Observation mode
- fixed angles
- Comments
- Emitted x-rays are collected in a solid angle directed at 90 degrees from the incident beam.
- Observation mode
- single spot
- Date begin - end
- 2017-02-15 - 2017-02-21
Versions
- Release date
- 2022-10-10 20:15:24 UTC+0000
- Version (Date)
- #1 (2022-10-10 20:15:24 UTC+0000, Updated: 2022-10-10 20:15:24 UTC+0000)