- Title
- Zn K edge XAS HERFD of Zn compounds at 10K for coordination determination in complex biological systems
- DOI
- 10.26302/SSHADE/EXPERIMENT_ST_20180418_001
- Data reference
- Thomas, Sara; Mishra, Bhoopesh (2018): Zn K edge XAS HERFD of Zn compounds at 10K for coordination determination in complex biological systems. SSHADE/FAME (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_ST_20180418_001
- Publications
- Database(s)
- Experimentalists
- Type(s)
- laboratory measurement
- Number of spectra
- 11
- Variable type(s)
-
- sample composition
- Instrument
- High Energy Resolution Fluorescence Detection X-ray Absorption Spectroscopy
- Sample holder
- ESRF helium mini-cryostat
- Standard medium
- unknown
- Observation mode
- spectrum
- Spectral range type(s)
- hard X
- Valid spectral range(s)
-
Min - Max ($eV$) Sampling ($eV$) Resolution ($eV$) Position accuracy ($eV$) Absorption edge #1 9512.0 - 10402.0 0.495 $Zn$ (K: 9.6586 $keV$) - Comments
- The resolution in the above table is the resolution given by the monochromator. The energy was calibrated by measuring the absorption edge of a reference: Zn metallic foil (first maximum of the derivative set at 9659 eV). The resolution of the spectrometer analyser was 1.4 eV (FWHM of the elastic peak).
Definition: emergence angle is positive with origin at nadir. Azimuth origin (increasing clockwise) is arbitrary.
- Observation geometry
- directional
- Observation mode
- fixed angles
- Comments
- Emitted x-rays are collected in a solid angle directed at 90 degrees from the incident beam.
- Observation mode
- averaged
- Date begin
- 2018-04-18
Versions
- Release date
- 2019-09-02 09:17:01 UTC+0000
- Version (Date)
- #1 (2019-09-02 09:17:01 UTC+0000, Updated: 2023-08-21 15:34:53 UTC+0000)