Pb L3 edge XAS fluorescence of lead(II) solution at hydrothermal conditions: PbS(s) in 1m NaHS + 2.2mg S (ESRF-Sol7) at 800 bar and 311°C

Spectrum

Title: Pb L3 edge XAS fluorescence of lead(II) solution at hydrothermal conditions: PbS(s) in 1m NaHS + 2.2mg S (ESRF-Sol7) at 800 bar and 311°C

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Data

Unit: Range: Valid spectral range(s): 103618042.963125 - 108207337.463477 eV

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References

DOI

10.26302/SSHADE/EXPERIMENT_DT_20170215_001

Data reference

Testemale, Denis; Brugger, Joel; Etschmann, Barbara; Liu, Weihua (2017): Pb L3 edge XAS fluorescence of lead(II) solution at hydrothermal conditions: 800 bar, 30 to 489°C. SSHADE/FAME (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_DT_20170215_001

Publications

Owner

Database

FAME

Experimentalists

Spectrum type

Experiment type: laboratory measurement
Type: fluorescence emission
Intensity unit: AU

Instrument #1

Instrument: X-ray Absorption Spectroscopy measured in fluorescence mode
Sample holder: Institut Néel autoclave, see Testemale et al., Rev. Sci. Instrum., 2005.

Spectral parameters

Standard medium

unknown

Observation mode

spectrum

Spectral range type(s)

hard X

Excitation wavelength

hard X

Valid spectral range(s)

	Min - Max ($eV$)	Sampling ($eV$)	Resolution ($eV$)	Position accuracy ($eV$)	Absorption edge
#1	12847.0 - 13416.0		0.668		$Pb$ (L3: 13.0352 $keV$)

Comments

The resolution in the above table is the resolution given by the monochromator. The energy was calibrated by measuring the absorption edge of a reference: Pb metallic foil (first maximum of the derivative set at 13035 eV).