Zn K edge XAS HERFD of aqueous Zn(Histidine)4 at 10K

Spectrum

Title: Zn K edge XAS HERFD of aqueous Zn(Histidine)4 at 10K

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Data

Unit: Range: Valid spectral range(s): 76719453.9320657 - 83897788.0363065 eV

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References

DOI

10.26302/SSHADE/EXPERIMENT_ST_20180418_001

Data reference

Thomas, Sara; Mishra, Bhoopesh (2018): Zn K edge XAS HERFD of Zn compounds at 10K for coordination determination in complex biological systems. SSHADE/FAME (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_ST_20180418_001

Publications

Owner

Database

FAME

Experimentalists

Spectrum type

Experiment type: laboratory measurement
Type: fluorescence emission
Intensity unit: AU

Instrument #1

Instrument: High Energy Resolution Fluorescence Detection X-ray Absorption Spectroscopy
Sample holder: ESRF helium mini-cryostat

Spectral parameters

Standard medium

unknown

Observation mode

spectrum

Spectral range type(s)

hard X

Excitation wavelength

hard X

Valid spectral range(s)

	Min - Max ($eV$)	Sampling ($eV$)	Resolution ($eV$)	Position accuracy ($eV$)	Absorption edge
#1	9512.0 - 10402.0		0.495		$Zn$ (K: 9.6586 $keV$)

Comments

The resolution in the above table is the resolution given by the monochromator. The energy was calibrated by measuring the absorption edge of a reference: Zn metallic foil (first maximum of the derivative set at 9659 eV). The resolution of the spectrometer analyser was 1.4 eV (FWHM of the elastic peak).